Applications of NMR Spectroscopy is a book series devoted to publishing the latest advances in the applications of nuclear magnetic resonance (NMR) spectroscopy in various fields of organic chemistry, biochemistry, health and agriculture.
The ninth volume of the series features reviews that highlight NMR spectroscopic techniques in microbiology, food science, pharmaceutical analysis and cancer diagnosis.
The ninth volume of the series features reviews that highlight NMR spectroscopic techniques in microbiology, food science, pharmaceutical analysis and cancer diagnosis.
The reviews in this volume are:
- NMR spectroscopy for the characterization of photoprotective compounds in cyanobacteria
- Coffee assessment using 1H NMR spectroscopy and multivariate data analysis: a review
- Evaluation of structure-property relationship of coconut shell lignins by NMR spectroscopy: from biorefinery to high-added value products
- Application of NMR spectroscopy in chiral recognition of drugs
- NMR-based metabolomics: general aspects and applications in cancer diagnosis
Table of Contents
Chapter 1 Nmr Spectroscopy For The Characterization Of Photoprotective Compounds In Cyanobacteria- Abha Pandey, Neha Kumari, Sonal Mishra, Jyoti Jaiswal And Rajeshwar P. Sinha 1 Introduction
- Principal Photoprotective Compounds In Cyanobacteria
- Mycosporine-Like Amino Acids (Maas)
- Scytonemin
- Nmr Spectroscopy
- One-Dimensional (1D) Nmr Spectroscopy
- 1H Nmr Spectroscopy
- 13C Nmr Spectroscopy
- 15N Nmr Spectroscopy
- 31P Nmr Spectroscopy
- 2D-Nmr Spectroscopy
- Correlation Spectroscopy (Cosy)
- Total Correlation Spectroscopy (Tocsy)
- 2D J-Resolved Spectroscopy (J-Res)
- Heteronuclear Single Quantum Correlation Spectroscopy (Hsqc)
- Heteronuclear Multiple Bond Correlation (Hmbc) Spectroscopy
- Some More Nmr Techniques Used In Metabolite Identification
- High-Resolution Magic-Angle Spinning Nmr Spectroscopy (Hrmas)
- Hyperpolarisation Methods
- Dynamic Nuclear Polarization (Dnp)
- Parahydrogen-Induced Polarisation (Phip) And Signal Amplification By Reversible Exchange (Sabre)
- Fast Nmr Methods
- Pure-Shift Nmr
- Lc-Nmr And Other Hybrid Nmr Approaches
- Applications Of Nmr In Metabolites
- Identification And Detection Of Metabolite Structures
- Stable Isotope Tracer Studies
- Cell-Based Tracing
- In Vivo Spectroscopic Measurements
- Nmr Is Used To Trace The Stable Isotope Labeling Or Isotopomer Study At Specified Atomic Positions
- Purity Determination Of Molecules
- To Check The Quality And Drug Findings Through The Natural Products
- Qualitative And Quantitative Analysis Of Food
- Nmr Spectroscopy In Structural Elucidation Of The Uv-Protective Pigment Scytonemin
- Extraction And Purification Of Scytonemin
- Nmr Procedure
- Conclusion
- Consent For Publication
- Conflict Of Interest
- Acknowledgements
- References
Chapter 2 Coffee Assessment Using 1H Nmr Spectroscopy And Multivariate Data Analysis: A Review
- Aline Coqueiro, Michel R. Baqueta, Manuela Mandrone, Ferruccio Poli And Patrícia Valderrama
- Introduction
- Authentication/Varieties Discrimination
- Authentication/Adulteration
- Authentication/Geographical Origin
- Sensory Classification Of Coffee
- Other Applications Of Metabolomics In Coffee
- Concluding Remarks
- Consent For Publication
- Conflict Of Interest
- Acknowledgements
- References
Chapter 3 Evaluation Of Structure-Property Relationship Of Coconut Shell Lignins By Nmr Spectroscopy: From Biorefinery To Highadded Value Products
- Francisco Avelino And Diego Lomonaco
- Introduction To The Lignin Chemistry
- Structural Elucidation Of Lignin By Nuclear Magnetic Resonance (Nmr)
- Biorefinery
- The Main Lignin Extraction Processes
- The Influence Of Pulping Parameters On The Lignin Structure
- Tuning The Lignin Functionalities In A One-Pot Process By Using Different Green Solvents
- General Features Of The Mwaod Process
- 1H Nmr
- 1H-13C Hsqc
- 31P Nmr
- Scale-Up Of Microwave-Assisted Organosolv Delignification Process: Nmr As A Quality Control Tool
- 1H Nmr
- 1H - 13C Hsqc
- 31P Nmr
- Practical Uses Of Nmr In Lignin Valorization
- Lignin-Based Epoxy Resins: Monitoring The Glycidylation Reaction And Quantification Of Oxirane Rings By Nmr
- Microwave-Assisted Phosphorylation Of Organosolv Lignin: Potential Bio-Additives For Epoxy Resins Formulations
- Microwave-Assisted Selective Acetylation Of Lignin As An Eco-Designed Process For Producing A Valuable Material With Several Technological Applications
- Final Considerations
- Consent For Publication
- Conflict Of Interest
- Acknowledgements
- References
Chapter 4 Application Of Nmr Spectroscopy In Chiral Recognition Of Drugs
- Vinod Kumar Vashistha, Sonika Sethianuj Kumar, Saeed Ahmed And Dipak , Kumar Das Objective:
- Introduction
- Background
- Method
- Application
- Introduction
- Chiral Solvating Agents (Csas)
- (Ii). Chiral Lanthanide Shift Reagents (Clsr)
- (Iii). Chiral Derivatizing Agents (Cdas)
- Scope Of The Present Chapter
- Chirality Recognition Of Chiral Pharmaceuticals
- Rasagiline
- Baclofen
- Betaxolol
- Ibuprofen
- Other Carboxylic Groups Containing Drugs
- Conclusion
- Consent For Publication
- Conflict Of Interest
- Acknowledgements
- References
Chapter 5 Nmr-Based Metabolomics: General Aspects And Applications In Cancer Diagnosis
- Jeferson Santana Ursulino, Alessandre Carmo Crispim, Lucas Monteiro Freire, Elton Rafael Castro Silva Matos, Jorge Artur Peçanha De Miranda Coelho, Manoel Alvaro Lins, Neto Edeildo Ferreira Da Silva Júnior And Thiago Mendonça De Aquino Systems Biology, Metabolome And Metabolomics
- Systems Biology
- Metabolome
- Metabolomics
- Nmr-Based Metabolomics
- Sample Collection
- Phosphate Buffer Solution Containing 3-Trimethyl-Silylpropionic Acid-D4 Sodium Salt (Tsp)
- Sample Preparation
- Serum And Blood Plasma
- Urine
- Fecal Water
- Nuclear Magnetic Resonance (Nmr)
- 1H Nmr - Internal Reference, Water Suppression And Spectral Data Processing
- Metabolite Identification
- 2D Nmr
- Statistical Analysis
- Principal Component Analysis (Pca)
- Partial Least Squares - Discriminant Analysis (Pls-Da)
- Orthogonal Partial Least Squares - Discriminant Analysis (Opls-Da)
- 1H Nmr-Based Metabolomics Associated With Cancer
- Breast Cancer
- Pancreatic Cancer
- Lung Cancer
- Colorectal Cancer
- Final Considerations
- Funding
- Conflict Of Interest
- Acknowledgements
- References
- Subject Index
Author
- Atta-ur-Rahman
- M. Iqbal Choudhary
