Metal-organic Frameworks in Analytical Sample Preparation and Sensing presents all the areas of applications of metal-organic frameworks in analytical sample preparation. Metal-organic frameworks are crystalline coordination polymers with robust and stable crystal structures, high synthetic tunability, and interesting properties for their use in analytical applications, including their detailed use as sorbents in miniaturized-extraction procedures and as components in sensors. This book also provides important information about the synthesis and characterization of these materials, with useful tips written by experts on the subject with respect to their conditioning, handling, and recycling. Their outstanding properties, adsorptive capabilities, and structural diversity are also highlighted. This will help experts in the field to select the proper metal-organic framework for a particular analytical application.
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Table of Contents
Section 1: Reticular materials: synthesis, characterization, and properties 1. Introduction and general aspects of metal-organic frameworks and other novel reticular materials 2. Synthesis of metal-organic frameworks with interest in analytical chemistry 3. Synthesis of covalent-organic frameworks with interest in analytical chemistry 4. Synthesis of composites based on reticular materials with interest in analytical chemistry Section 2: Metal-organic frameworks as sorbents in analytical sample preparation 5. Metal-organic frameworks in micro-solid phase extraction 6. Metal-organic frameworks in micro-dispersive solid phase extraction and stir bar sorptive extraction 7. Metal-organic frameworks in magnetic-based methods 8. Metal-organic frameworks in solid-phase microextractionIncludes both in-fiber and in-tube solid-phase microextraction 9. Metal-organic frameworks in thin film microextraction 10. Hyphenating microextraction methods based on metal-organic frameworks with chromatographic techniques Section 3: Metal-organic frameworks as sensors for analysis 11. Metal-organic frameworks as luminescence sensors 12. Metal-organic frameworks as electrochemical sensors 13. Other sensing applications of metal-organic frameworks Section 4: Novel reticular materials in analytical sample preparation and sensing 14. Covalent-organic frameworks in sample preparation 15. Covalent-organic frameworks as sensors for analysis