Microscale Organic Chemistry: With Multistep and Multiscale Syntheses offers a modern approach to the laboratory experience within the organic division. Notable features include inquiry-driven experimentation, validation of the purification process, and the implementation of greener processes (including microwave use) to perform traditional experimentation. In addition to offering alternative methods to perform microscale experiments, this text offers strong pedagogy to promote student success through empowerment and encouragement.
Table of Contents
Chapter 1 Introduction 1
Chapter 2 Safety 6
Chapter 3 Introduction to Microscale Organic Laboratory Equipment And Techniques 20
Chapter 4 Determination of Physical Properties 47
Chapter 5 Microscale Laboratory Techniques 59
Chapter 6 Microscale Organic Laboratory Experiments 119
Chapter 7 Sequential Syntheses: the Transition From Macro To Micro 440
Chapter 8 Spectroscopic Identification The Monochromator 625
Chapter 9 Qualitative Identification Of Organic Compounds 649
Chapter 10 Advanced Microscale Organic Laboratory Experiments 685
Glossary G-1
Index I-1